In this article,a method is developed to determine the terpene components in the essential oil of cedarwood, with HP-5MS crossed silicon capillary column,and the temperature program:120 ℃2 ℃/min 200 ℃.
采用毛细管气相色谱法 (CGC)分析了柏木精油中萜烯成分 ,色谱条件 :HP - 5MS( 3 0m× 0 。
The major components of cedar wood oil including some isomers α-cedrene, β-cedrene, thujopsene and so on,were separated by GC/MS and 19 compounds were identified.
本文利用GC/MS技术,对柏木油中的主要产物α—柏木烯、β—柏木烯、罗汉柏烯等同分异构体进行分离定性,共定出19个组份。
32g cedrol extracted from cedar wood oil,176ml dried dimethyl benzene and 7g aminosodium,the reactants were refluxed for 2h at 115~125℃.
由柏木油中提取的柏木醇32g、176ml二甲苯、氨基钠7g,在115~125℃下回流2h,冷却,慢慢滴加32g硫酸二乙酯,在115~125℃回流1h,分馏,在113~114℃/0。
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